摘要
用熔融法制备了花岗岩废渣微晶玻璃。采用差示扫描量热法(DSC)、X-射线衍射(XRD)、扫描电子显微镜(SEM)等测试方法研究了CaO对微晶玻璃结构及性能的影响。结果表明:CaO取代量为0%时,试样中晶相为铁板钛矿,透辉石、镁橄榄石;随着CaO取代量增加到4%,试样中晶相为透辉石相,铁板钛矿,试样的力学性能最为优异(CaO取代量0~6%),抗弯强度和显微硬度分别为142.53 MPa、6.97 GPa。
Granite residual glass-ceramics were prepared by melting technique. The effects of CaO on the structure and properties of glass-ceramics were investigated by differential scanning calorimetry(DSC),X-ray diffraction(XRD) and scanning electron microscopy(SEM). The results showed that when the CaO substitution content was 0%, the crystalline phases of the sample were pseudobrookite, diopside and forsterite; as the CaO substitution content increased to 4%, the crystalline phases of the sample were pseudobrookite and diopside, the sample exhibited the most excellent mechanical properties( CaO substitution 0~6%), and the flexural strength and microhardness were 142.53 MPa and 6.97 GPa,respectively.
引文
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