摘要
与过去传统的农药残留样品前处理技术相比,近年来,农药残留检测技术向着过程简单化、微型化和自动化的方向发展。综述了几种近年来常用的农药残留样品前处理新技术,并对样品前处理技术进行了展望,以期为中药材的农药残留检测的样品前处理技术提供一定的参考。
In recent years, the developmental trend of pesticide residues detection technology is characterized by simplification,miniaturization and automation during sample pretreatment process. In this paper, several newly used sample pretreatment techniques for pesticide residues detection in recent years were reviewed and prospected, in hoping to provide references for the development of sample pretreatment method of pesticide residues detection in traditional Chinese medicine.
引文
[1]高倩,花日茂,汤锋,等.中药材农药残留研究现状[J].安徽农业科学,2008,36(23):10147-10151.
[2]关美琳,郎朗.农药残留分析检测中的样品前处理技术的研究进展[J].黑龙江医药,2015(2):245-247.
[3]刘嫦娥,胡波,吴敏,等.农产品农药残留的危害与预防[J].现代农业科技,2012(14):290.
[4]江泽军,张鹏,李永飞,等.分散固相萃取—高效液相色谱—串联质谱法测定水稻和土壤中的福美双与甲霜灵残留[J].农药学学报,2015(3):313-320.
[5]张桂云,杨伟强,林振宇.分散固相萃取—超高效液相色谱串联质谱法检测水产品中多兽药残留[J].福州大学学报(自然科学版),2019,47(3):424-429.
[6]申书昌,任芳秀,吕伟超.镍钛合金纤维/有机硅—聚氨酯固相微萃取头的制备及其在水中7种取代苯化合物检测中的应用[J].色谱,2018,36(12):1323-1329.
[7]滕晓宇,李建勋,胡雪艳,等.分散固相萃取结合气相色谱—四极杆—飞行时间质谱测定茶叶中13种三唑类农药残留[J/OL].食品科学技术学报:1-9[2019-04-16].http://kns.cnki.net/kcms/detail/10.1 151.TS.20190405.1606.002.html.
[8]罗庆,王诗雨,单岳,等.固相微萃取—气相色谱/质谱联用技术测定水样中13种有机磷酸酯[J].分析科学学报,2018,34(6):751-756.
[9]张悦,袁骐,黄冬梅,等.固相萃取—气相色谱法检测海水中邻苯二甲酸二丁酯[J/OL].分析试验室:1-5[2019-04-16].https://doi.org/10.13595/j.cnki.issn 1000-0720.2018.061302.
[10]王伟.基质固相分散—快速溶剂萃取-GC/M5法同时测定土壤中有机氯农药和多环芳烃[J].中国环境监测,2019,35(1):135-141.
[111]秦伟瀚,阳勇,师萱,等.基质分散固相萃取法同时检测13种不同产地昆明山海棠中有机磷和拟除虫菊酯类农药残留[J].重庆中草药,2017,37(7):613-616.
[12]ME YE A,WOLFGANG K,KARL C.SPE of PAHs from solids with a high carbon content and analyte collection via com-bined liquid/solid trapping[J].Journal of High Resolution Chromatography,1993,16(8):491-493.
[13]桂文龙,苏治国,李巨银.超临界萃取技术提取土茯苓中总黄酮的研究[J].黑龙江畜牧兽医,2018(12):184-187.
[14]于飞飞,郐鹏,周宏霞,等.基于QuEChERS净化—气相色谱法检测樱桃中16种有机氯及拟除虫菊酯类农药残留[J].农药,2018,57(5):340-342.
[15]王姣.QuEChERS-气相色谱—串联质谱法测定茶叶中的多种拟除虫菊酯农药[J].现代食品,2018(15):121-125.
[16]丁润梅,吴冰,田大年,等.QuEChERS-气相色谱—质谱联用法测定温棚蔬菜中7种氨基甲酸酯及5种拟除虫菊酯农药残留[J].现代预防医学,2018,45(17):3160-3164.