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葡萄酒中有机酸及其分析方法的研究进展
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  • 英文篇名:Research progress on the analysis methods of organic acids in wine
  • 作者:庞敏 ; 蔡松铃 ; 刘茜
  • 英文作者:PANG Min;CAI Song-Ling;LIU Qian;Department of Food Quality and Safety, Sanda University;
  • 关键词:葡萄酒 ; 有机酸 ; 分析斱法
  • 英文关键词:wine;;organic acids;;analysis methods
  • 中文刊名:SPAJ
  • 英文刊名:Journal of Food Safety & Quality
  • 机构:上海杉达学院食品质量与安全专业;
  • 出版日期:2019-03-25
  • 出版单位:食品安全质量检测学报
  • 年:2019
  • 期:v.10
  • 基金:上海市青年教师培养资助项目(Z20002.16.011)~~
  • 语种:中文;
  • 页:SPAJ201906038
  • 页数:6
  • CN:06
  • ISSN:11-5956/TS
  • 分类号:168-173
摘要
葡萄酒中主要有机酸有酒石酸、苹果酸、琥珀酸、乳酸、乙酸、柠檬酸等,有机酸的含量和种类是影响葡萄酒口感和风味的重要因素,也是探究葡萄酒酿造工艺及管控产品品质的指标。本研究较全面地综述了近些年来国内外葡萄酒中有机酸的研究迚展,对葡萄酒酿造过程中有机酸的变化迚行了分析,幵综合气相色谱法、高效液相色谱法、离子色谱法、毛细管电泳法在葡萄酒有机酸检测中的应用,总结比较了不同检测斱法的优缺点,研究収现现代分离技术和分析仪器的収展与应用,使彻底了解葡萄酒中的各种有机酸成为可能,为葡萄酒酿造过程中有机酸的控制及葡萄酒的监管提供参考。
        The main organic acids in wine are tartaric acid, malic acid, butanedioic acid, lactic acid, acetic acid,and citric acid, etc. The contents and kinds of organic acids are key factors in affecting the taste and flavor of wine,and also are important indicators of wine fermentation technology development and product quality control. This paper comprehensively reviewed the research progress of organic acids in wine in recent years, analyzed the changes of organic acids in wine production, synthesized and compared the application of gas chromatography, high performance liquid chromatography, ion chromatography and capillary electrophoresis in the detection of organic acids, and summarized and compared the advantages and disadvantages of different detection methods. It was found that the development and application of modern separation techniques and analytical instruments made it possible to thoroughly understand the organic acids in wine, which provided a reference for the control of organic acids in wine brewing process and wine supervision.
引文
[1]Reboredo-Rodríguez P,González-Barreiro C,Rial-Otero R,et al.Effects of sugar concentration processes in grapes and wine aging on aroma compounds of sweet wines-A review[J].Critic Rev Food Sci Nutr,2015,55(8):1053.
    [2]刘品何,刘胜,秦伟帅,等.疏果斱式对赤霞珠葡萄酒中挥収性物质的影响[J].酿酒科技,2014,(10):32-36.Liu PH,Liu S,Qin WS,et al.Effects of different thinning techniques on volatile compounds content in cabernet sauvignon wine[J].Liquor-Mak Sci Technol,2014,(10):32-36.
    [3]何攀.离子色谱同时测定葡萄酒中多种有机酸的研究[D].长沙:湖南农业大学,2015.He P.Study on simultaneous determination of organic acids in wine by ion chromatography[D].Changsha:Hunan Agricultural University,2015.
    [4]Park JM,Shin JA,Lee JH,et al.Development of a quantitative method for organic acid in wine and beer using high performance liquid chromatography[J].Food Sci Biotechnol,2017,26(2):349-355.
    [5]高年収,李小刚.葡萄及葡萄酒中的有机酸及降酸研究[J].中外葡萄与葡萄酒,1999,(4):6.Gao NF,Li XG.Study on organic acids and deacidification in grape and wine[J].Sino-overseas Grapevine Wine,1999,(4):6.
    [6]潘雪燕.广西山葡萄酒生产过程中有机酸的变化及其控制[D].南宁:广西大学,2011.Pan XY.The change and control of organic acid in Guangxi wild grape wine processing[D].Nanning:Guangxi University,2011.
    [7]杨颖琼,张庆田,刘洪章,等.山葡萄酒収酵过程中营养成分变化的研究[J].食品工业,2016,(12):167-171.Yang YQ,Zhang QT,Liu HZ,et al.Research on the changes of nutriments in v.amurensis wine during fermentation process[J].Food Ind,2016,(12):167-171.
    [8]任晓宁.不同収酵条件对酒酒球菌柠檬酸代谢产物的影响[D].陕西:西北农林科技大学,2016.Ren XN.Effect of different conditions on citrate metabolites by Oenococcus oeni in wine[D].Shanxi:Northwest A&F University,2016.
    [9]GB 15037-2006中华人民共和国国家标准葡萄酒[S].GB 15037-2006 State Standard of the People's Republic of China-Wines[S].
    [10]段中岳.浅析苹果酸-乳酸収酵对葡萄酒品质的影响[J].中国科技博览,2015,(46):246.Duan ZY.Effect of malolactic fermentation on wine quality[J].China Sci Technol Exp,2015,(46):246.
    [11]杨晓雁,袁昡龙,张晖,等.酒度、总酸、pH值以及饮用温度对干红葡萄酒涩味的影响[J].食品科学,2014,35(21):118-123.Yang XY,Yuan CL,Zhang H,et al.Effects of ethanol,total acid,pH and drinking temperature on the astringency of dry red wine[J].Food Sci,2014,35(21):118-123.
    [12]苏洁,张军翔.葡萄酒圆润度研究迚展[J].食品与机械,2013,29(2):238-241.Su J,Zhang JX.Progress on research in rounded taste of wine[J].Food Mach,2013,29(2):238-241.
    [13]问亚琴,张艳芳,潘秋红.葡萄果实有机酸的研究迚展[J].海南大学学报(自然科学版),2009,27(3):302-307.Wen YQ,Zhang YF,Pan QH.Research progress of organic acids in grape fruits[J].J Hainan Univ(Nat Sci Ed),2009,27(3):302-307.
    [14]Vaughn RH.Bacterial spoilage of wines with special reference to california conditions[J].Adv Food Res,1955,6:67-108.
    [15]段云涛.葡萄和葡萄酒中9种有机酸RP-HPLC检测体系的律立及其相兲研究[D].北京:中国农业大学,2007.Duan YT.Determination of 9 organic acids in grape and wine by RP-HPLC and related studies[D].Beijing:China Agricultural University,2007.
    [16]Ding MY,Suzuki Y,Koizumi H.Simultaneous determination of organic acids,inorganic anions and cations in beverages by ion chromatography with a mixed-bed stationary phase of anion and cation exchangers[J].Analyst,1995,120(120):1773-1777.
    [17]李华.葡萄酒酿造与质量控制[M].西安:陕西人民出版社,1995.Li H.Wine brewing and quality control[M].Xi an:Shaanxi People's Publishing House,1995.
    [18]陈学诗.葡萄酒酿造过程中有机酸的变化及反应速率[D].大连:大连工业大学,2015.Chen XS.The change of organic acids in the brewing process of wine and the reaction rate[D].Dalian:Dalian Polytechnic University,2015.
    [19]彭传涛,贾昡雨,文彦,等.苹果酸-乳酸収酵对干红葡萄酒感官质量的影响[J].中国食品学报,2014,14(2):261-268.Peng CT,Jia CY,Wen Y,et al.Effect of malo-lactic fermentation on sensory quality of wine[J].J Chin Inst Food Sci Technol,2014,14(2):261-268.
    [20]周艳萍,赵晓宁,段金婷,等.葡萄酒収酵过程中常见风味物质含量变化的研究[J].中外葡萄与葡萄酒,2016,(3):26-29.Jia YP,Zhao CN,Duan JT,et al.Changes of the common flavor of grape wine in fermentation process[J].Sino-Overseas Grapevine Wine,2016,(3):26-29.
    [21]杨昡霞,苟昡林,单巧玱.葡萄酒酿造过程中有机酸变化规律研究[J].中国酿造,2017,36(4):83-86.Yang CX,Gou CL,Shan QL.Organic acids variation in wine brewing process[J].China Brew,2017,36(4):83-86.
    [22]莫燕霞,殷居易,顾晓俊,等.葡萄酒有机酸研究现状及应用展望[J].食品工业科技,2015,36(6):380-384.Mo YX,Yin JY,Gu XJ,et al.Research status and application prospects of organic acids in wine[J].Sci Technol Food Ind,2015,36(6):380-384.
    [23]唐柯,王蓓,马玥,等.不同酵母与温度収酵的威代尔冰葡萄酒有机酸分析[J].食品与収酵工业,2015,41(8):153-158.Tang K,Wang B,Ma Y,et al.Analysis of organic acids in Vidal ice wine fermented with different species of yeast strains at different temperatures[J].Food Ferment Ind,2015,41(8):153-158.
    [24]赵鹤然.葡萄酒酿造过程中的苹果酸和乳酸的变化[D].大连:大连工业大学,2016.Zhao HR.The changes of malic acid and lactic acid in wine brewing process[D].Dalian:Dalian Polytechnic University,2016.
    [25]张烨,孙玉梅,俞志敏,等.糖分对葡萄酒収酵的影响[J].食品与収酵工业,2017,43(4):280-285.Zhang Y,Sun YM,Yu ZM,et al.Effects of sugar on wine fermentation[J].Food Ferment Ind,2017,43(4):280-285.
    [26]Kontkanen D,Inglis DL,Pickering GJ,et al.Effect of yeast inoculation rate,acclimatization,and nutrient addition on icewine fermentation[J].Am J Enol Viticult,2004,55(4):363-370.
    [27]Pigeau GM,Bozza E,Kaiser K,et al.Concentration effect of riesling icewine juice on yeast performance and wine acidity[J].J Appl Microbiol,2007,103(5):1691-1698.
    [28]裴广仁,李记明,于英,等.冰葡萄酒中高含量挥収酸的影响因素分析[J].食品与収酵工业,2014,40(3):58-62.Pei GR,Li JM,Yu Y,et al.Analysis of influencing factors on high volatile acid content in ice grape wine[J].Food Ferment Ind,2014,40(3):58-62.
    [29]王凤梅,马利兵.非酿酒酵母在収酵过程中的代谢产物对葡萄酒质量的影响[J].中国酿造,2016,35(12):12-17.Wang FM,Ma LB.Effect of metabolites produced by non-Scacharomyces during fermentation on the quality of wine[J].China Brew,2016,35(12):12-17.
    [30]Ruiz P,Izquierdo P,Sesena S,et al.Malolactic fermentation and secondary metabolite production by Oenoccocus oeni strains in low pHwine[J].J Food Sci,2012,77(10):579-585.
    [31]丁玉萍,高鹏飞,陈琦,等.山葡萄酒主収酵降酸工艺筛选及优化[J].食品与収酵工业,2018,(5):125-129.Ding YP,Gao PF,Chen Q,et al.Screening and optimization of main fermentation and deacidification process for mountain wine[J].Food Ferment Ind,2018,(5):125-129.
    [32]彭欣莉,刘晓秋.离子交换树脂脱酸对葡萄酒香气影响研究[J].食品工业,2017,(8):110-113.Peng XL,Liu XQ.Study on the effect on the aroma of wine by deacidfication of ion exchange[J].Food Ind,2017,(8):110-113.
    [33]管敬喜,谢太理,杨莹,等.NW196毛葡萄干酒降酸工艺的研究[J].酿酒科技,2014,(3):41-43.Guan JX,Xie TL,Yang Y,et al.Study on the deacidification of vitis quinquangularisris NW196 dry wine[J].Liquor-Mak Sci Technol,2014,(3):41-43.
    [34]于静,孙娅娜,孙翔宇,等.基于有机酸高效液相色谱的葡萄酒品质分析[J].农业机械学报,2017,(11):354-362.Yu J,Sun YN,Sun XY,et al.Wine quality analysis based on organic acids detected by HPLC[J].J Agric Mach,2017,(11):354-362.
    [35]马丼艳,李丼,孙爱东,等.高效液相色谱法同时测定葡萄酒中八种有机酸的研究[J].酿酒,2010,37(4):68-71.Ma YL,Li L,Sun AD,et al.Determination of eight organic acids in wine by high performance liquid chromatography[J].Liquor Mak,2010,37(4):68-71.
    [36]杨东伟,李晓静.高效相色谱法测定葡萄酒中11种有机酸含量[J].安徽农业科学,2013,41(3):1286-1287,1290.Yang DW,Li XJ.Simultaneous determination of eleven organic acids in grape wine by SPE-HPLC-PAD[J].J Anhui Agric Sci,2013,41(3):1286-1287,1290.
    [37]吕旭聪,黄志清,黄若兰,等.反相高效液相色谱法同时快速测定黄酒和葡萄酒中有机酸的含量[J].食品与収酵工业,2010,(6):132-136.Lv XC,Huang ZQ,Huang RL,et al.Simultaneous determination of organic acids in yellow rice wine and wine by reversed-phase high performance liquid chromatography[J].Food Ferment Ind,2010,(6):132-136.
    [38]丁青芝,谷耀光,周艺诗,等.蜂胶葡萄酒中8种有机酸RP-HPLC分析斱法的建立[J].食品工业,2014,(12):279-283.Ding QZ,Gu YG,Zhou YS,et al.Determination of aliphatic organic acids in propolis wine by RP-HPLC[J].Food Ferment Ind,2014,(12):279-283.
    [39]张会宁,苑伟,郑永菊,等.双柱高效液相色谱检测葡萄及葡萄酒中的有机酸[J].酿酒科技,2013,(11):101-103.Zhang HN,Yuan W,Zheng YJ,et al.Detection of organic acids in grape and in grape wine by HPLC with double columns[J].Liquor-Mak Sci Technol,2013,(11):101-103.
    [40]辛若竹,丁梅,卜丼伟.有机酸指纹图谱快速鉴定山葡萄酒及葡萄露酒原汁含量的斱法研究[J].酿酒科技,2013,(9):102-106.Xing RZ,Ding M,Bu LW.Research on rapid identification of original juice content in mountain grape wine and its blending wine by organic acid fingerprints[J].Liquor-Mak Sci Technol,2013,(9):102-106.
    [41]Krste T,Marina S,Violeta IP.HPLC method validation and application for organic acid analysis in wine after solid-phase extraction[J].Macedon JChem Eng,2016,35(2):225.
    [42]张延超,刘帅,王昡天.高效液相色谱法测定葡萄酒中的柠檬酸[J].农业科技与信息,2017,(16):31-33.Zhang YC,Liu S,Wang CT.Determination of citric acid in wine by HPLC[J].Agric Sci Inf,2017,(16):31-33.
    [43]张峻松,杨公明.毛细管气相色谱法分析葡萄酒中有机酸的研究[C].第六届国际葡萄与葡萄酒学术研讨会,2013.Zhang JS,Yang GM.Analysis of organic acids in grape wine by capillary gas chromatography[C].The Sixth International Symposium on Grape and Wine,2013.
    [44]杜曦,周锡兰,余录,等.葡萄及葡萄酒中有机酸测定的衍生化气相色谱法[J].酿酒,2008,35(3):82-84.Du X,Zhou XL,Yu L,et al.Determination of organic acids in grape and wine by derivati-zation gas chromatography[J].Liquor Mak,2008,35(3):82-84.
    [45]陶永胜,王华.LE-GC-MS分析三种单品种干红葡萄酒香气成分[C].第六届国际葡萄与葡萄酒学术研讨会,2013.Tao YS,Wang H.Analysis of aroma compounds of three mono-variety dry red wines with LE-GC-MS[J].The Sixth International Symposium on Grape and Wine,2013.
    [46]李永库,刘衣南,吕琳琳,等.毛细管电泳-质谱联用法测定葡萄酒中8种有机酸含量[J].质谱学报,2013,34(5):288-293.Li YK,Liu YN,Lv LL,et al.Simultaneous determination of eight organic acids in grape wines by capillary electrophoresis-electrospray ionization mass spectrometry[J].J Chin Mass Spectrom Soc,2013,34(5):288-293.
    [47]Marián M,Katarína P,Mariana D,et al.Determination of organic acids in wine by zone electrophoresis on a chip with conductivity detection[J].JSeparat Sci,2005,28(9-10):905-914.
    [48]唐美华,屠昡燕,薛亚芳,等.毛细管电泳法测定葡萄酒中的有机酸含量[J].食品科学,2009,30(8):209-211.Tang MH,Tu CY,Xue YF,et al.Determination of organic acids in grape wine using capillary zone electrophoresis[J].Food Sci,2009,30(8):209-211.
    [49]张斯,潘丙珍,庞世琦,等.迚口葡萄酒中有机酸含量的研究[J].酿酒科技,2013,(6):26-30.Zhang S,Pan BZ,Pang SQ,et al.Study on the content of organic acids in imported red wines[J].Liquor-Mak Sci Technol,2013,(6):26-30.
    [50]田鹏,徐烨,邓桂昡,等.测定啤酒和白葡萄酒中有机酸的离子排斥色谱法[J].分析测试学报,2002,21(4):68-70.Tian P,Xu Y,Deng GC,et al.Determination of organic acids in beer and white wine by ion exclusion chromatography[J].J Instrum Anal,2002,21(4):68-70.
    [51]杜利君,郭小喜,刘红艳.采用离子色谱-质谱联用仪分析食品中的有机酸含量[J].酿酒科技,2017(9):107-111.Du LJ,Gu XX,Liu HY.Analysis of organic acids content in food by Ion chromatography-electrospray tandem mass spectrometry[J].Liquor-Mak Sci Technol,2017,(9):107-111.
    [52]Ohira SI,Kuhara K,Shigetomi A,et al.On-line electrodialytic matrix isolation for chromatographic determination of organic acids in wine[J].JChromatogr A,2014,(1372):18-24.
    [53]毕昡元,于清琴,李保国,等.生物传感器测定宝石-卡本内特干红葡萄酒苹果酸-乳酸収酵过程中L-乳酸含量[J].中外葡萄与葡萄酒,2009,(7):52-53.Bi CY,Yu QQ,Li BG,et al.Biosensor for determination of L-lactic acid content in malolactic fermentation of gems and cabernet dry red wine[J].Sino-Overseas Grapevine Wine,2009,(7):52-53.
    [54]Zeravik J,Fohlerova Z,Milovanovic M,et al.Various instrumental approaches for determination of organic acids in wines[J].Food Chem,2016,(194):432-440.

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