摘要
本文建立了气相色谱法测定煤基费托合成粗液体蜡中的正构烷烃含量。该方法不需要对样品进行前处理,操作简单,检测过程准确高效,可以为煤基费托合成液体蜡生产过程及产品监管提供技术支撑。
This paper establishes a set of analysis method based on gas chromatograph to determine the contents of n-alkane in the crude liquid paraffin synthesized from coal-based Fischer-Tropsch reaction. The method featuring with ease of operation and accuracy and efficiency of detection does not need to pretreat samples. It can provide technical support for the synthesis process and final product supervision of coal-based Fischer-Tropsch reaction.
引文
[1]中华人民共和国国家质量监督检验检疫总局,中国国家标准化管理委员会.GB/T 32066-2015煤基费托合成液体蜡[S].北京:中国标准出版社,2015.
[2]中国石油化工总公司.SH/T 0410-1992液体石蜡及原料中正构烷烃含量及碳数分布测定法(气相色谱法)煤基费托合成液体蜡[S].北京:中国石化出版社,1992.
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[4]齐邦峰,程仲芊,张会成,祝馨怡,韩小茜,陈立仁.高温气相色谱法测定橡胶防护蜡中的正构烷烃和非正构烷烃[J].橡胶工业,2003,50(6):373-375.