异烟酰腙配体多孔配位聚合物的合成、结构与吸水—脱水性能研究
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摘要
(1)合成了2,3-丁二酮双缩异烟肼双Schiff碱配体的锰配位聚合物[MnL]_n·2nH_2O,解析了单晶结构。该配位聚合物具有由Mn-Mn通过桥联配体L中吡啶环上的N原子和Schiff碱亚胺的N原子连接形成的二维(4,4)网格结构。此二维(4,4)网格具有正方形格子。对这个配位聚合物进行了热重分析,IR谱分析,固体和DMF溶液的紫外-可见吸收光谱分析。
(2)以异烟肼、丁二酮和硝酸铈为原料,合成了新配合物[(CeL)(NO_3)_2(H_2O)_2]NO_3,首次得到了以丁二酮双缩异烟肼双Schiff碱为配体的铈配合物,解析了单晶结构,进行了IR谱分析和DMF溶液的紫外-可见吸收光谱分析。
(3)采用多种不同的方法处理配位聚合物{[ZnL](NO_3)_(0.5)(OH)_(0.5)}_n·1.5nH_2O的晶体,发现处理后得到的样品其颜色都有差异。该配位聚合物是亮黄色的晶体,部分失水(在空气中恒重)后为橙红色晶体,烘干至恒重后变为红色晶体,充分吸水后又变为黄色。该配位聚合物晶体经多种不同方法处理前后的固体紫外-可见光谱图显示,金属Zn和配体L间的电荷迁移跃迁最大吸收峰位置不同,而光谱的其余部分变化不大。
(1) A porous coordination polymer [MnL]_n·2nH_2O was synthesized. It has a 2,3-butanedione bisisonicotinoyl hydrazone as Schiff base ligand. The coordination polymer has a 2D(4, 4) square grid structure. The coordination polymer is characterized by TG-DTA, IR spectra, solid and solution UV-Vis spectra and X-ray single crystal diffraction.
(2) A crystalline complex [(CeL)(NO_3)_2(H_2O)_2]NO_3 was synthesized by mixing 2, 3-butanedione, isonicotinoyl hydrazine and Ce(NO_3)_3·6H_2O in CH_3OH/H_2O. The complex is characterized both by spectral methods and X-ray single crystal diffraction.
(3) The hydration-dehydration properties of the porous coordination polymer {[ZnL](NO_3)_(0.5)(OH)_(0.5)}_n·1.5nH_2O was investigated. It was found that the crystal has different colors under different conditions. The crystal is brilliant yellow. It partially loses water with the color changes to orange-red in the air. The color of the crystal turned red after being baked. The color turned brilliant yellow again after the sample being fully hydrated. The peak positions for the charge-transfer transition of samples with different hydration-dehydration levels were different, while the other parts of the spectra have little difference.
(2)以异烟肼、丁二酮和硝酸铈为原料,合成了新配合物[(CeL)(NO_3)_2(H_2O)_2]NO_3,首次得到了以丁二酮双缩异烟肼双Schiff碱为配体的铈配合物,解析了单晶结构,进行了IR谱分析和DMF溶液的紫外-可见吸收光谱分析。
(3)采用多种不同的方法处理配位聚合物{[ZnL](NO_3)_(0.5)(OH)_(0.5)}_n·1.5nH_2O的晶体,发现处理后得到的样品其颜色都有差异。该配位聚合物是亮黄色的晶体,部分失水(在空气中恒重)后为橙红色晶体,烘干至恒重后变为红色晶体,充分吸水后又变为黄色。该配位聚合物晶体经多种不同方法处理前后的固体紫外-可见光谱图显示,金属Zn和配体L间的电荷迁移跃迁最大吸收峰位置不同,而光谱的其余部分变化不大。
(1) A porous coordination polymer [MnL]_n·2nH_2O was synthesized. It has a 2,3-butanedione bisisonicotinoyl hydrazone as Schiff base ligand. The coordination polymer has a 2D(4, 4) square grid structure. The coordination polymer is characterized by TG-DTA, IR spectra, solid and solution UV-Vis spectra and X-ray single crystal diffraction.
(2) A crystalline complex [(CeL)(NO_3)_2(H_2O)_2]NO_3 was synthesized by mixing 2, 3-butanedione, isonicotinoyl hydrazine and Ce(NO_3)_3·6H_2O in CH_3OH/H_2O. The complex is characterized both by spectral methods and X-ray single crystal diffraction.
(3) The hydration-dehydration properties of the porous coordination polymer {[ZnL](NO_3)_(0.5)(OH)_(0.5)}_n·1.5nH_2O was investigated. It was found that the crystal has different colors under different conditions. The crystal is brilliant yellow. It partially loses water with the color changes to orange-red in the air. The color of the crystal turned red after being baked. The color turned brilliant yellow again after the sample being fully hydrated. The peak positions for the charge-transfer transition of samples with different hydration-dehydration levels were different, while the other parts of the spectra have little difference.
引文
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