海洋环境中金属材料现场电化学检测及冲刷腐蚀研究
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摘要
我国材料环境海水腐蚀试验网站的基础数据积累研究,已经获得了大量宝贵的腐蚀数据。国家自然科学基金重大项目“材料在自然环境腐蚀过程中原位实时监检测新技术的基础与应用研究”(No. 50499335,2004.9～2008.7)的主要研究内容为“水环境腐蚀站网典型金属材料暴露试件现场实时检测”。针对舟山海域海水泥沙含量大、海生物附着少的特点,对舟山海水腐蚀试验站暴露金属试片进行现场腐蚀电化学检测,研究了金属材料在模拟泥沙海水及实海冲刷环境下的腐蚀行为,为材料在海洋环境中腐蚀行为的研究及预测提供了依据。
实现了实海暴露金属试片的现场腐蚀电化学检测,恒电位方波和电化学阻抗谱(EIS)检测结果反映了试片在海水不同区带的腐蚀行为及海水环境因素的直接影响。确定了Q235钢、Q235超细晶钢、09CuPCrNiRE耐候钢和09CuPCrNi超细晶超高强度钢在海水中的极化阻力方程式的B值,为研究碳钢、低合金钢在海水中的腐蚀行为有很大意义。获得了实海试片暴露期间腐蚀速率的连续变化规律,碳钢、低合金钢全浸试片暴露1年和2年的电化学检测结果与失重结果一致。
采用灰关联分析法分析了暴露期间试片不同时间的腐蚀速度与海水环境因素(潮位、温度、流速和流向)的关系,结果表明:海水温度是影响全浸和潮差试片腐蚀速度的主要因素,海水潮位对潮差试片腐蚀速度的影响程度与温度的影响非常接近。
利用模拟冲刷腐蚀测试系统研究了3C、10CrMoAl、ZHMn55-3-1和HAl77-2在模拟泥沙海水冲刷条件下的腐蚀行为。模拟实海流速0~0.8m/s范围内,流速是影响3C和10CrMoAl腐蚀速度的主要因素,而泥沙含量的影响并不显著。流速和泥沙对ZHMn55-3-1和HAl77-2铜合金在模拟实海流速以及模拟高速下的冲刷腐蚀行为都有影响。
在舟山海水腐蚀试验站实现了金属材料的实海冲刷腐蚀电化学检测,检测结果表明:在流速1～3m/s范围内,3C、10CrMoAl和ZHMn55-3-1的腐蚀速度随流速的增加而增大,与实海冲刷腐蚀失重结果一致。材料的冲刷腐蚀形貌也进一步验证了电化学检测结果。
On the basis of China's material ambient seawater corrosion network test data accumulated, a great deal of valuable corrosion data has been obtained. National Natural Science Foundation of major projects "in situ material in a natural process of corrosion testing of new technology based on real-time monitoring and application" (No.50499335, 2004.9~2008.7), the main content of this project is "Water environment network typical metal corrosion specimens exposed real-time detection". Focused on the characteristics of Zhoushan seawater with larger concentration of sand and less marine organism, in field corrosion electrochemical detections of metal samples in Zhoushan marine corrosion test station have been implemented. The corrosion behaviors of metal samples both in simulated erosion-corrosion of seawater with sand and in marine erosion-corrosion conditions have been studied. These offer the foundation to investigate and forecast the corrosion performances of materials in marine environment.
The in field corrosion electrochemical detections of metal samples in marine environment have been achieved. Potentiostatic square wave and electrochemical impedance spectroscopy (EIS) results reflect the corrosion behaviors of metal samples exposed in different zone and the direct influence of marine environmental factors on the corrosion behaviors. The values of the parameter“B”in polarization resistance formula of Q235 carbon steel, Q235 ultrafine grained steel, 09CuPCrNiRE weathering steel and 09CuPCrNi ultrafine grained high strength steel have been identified, which have an great significance to investigate the corrosion behaviors o f carbon steels and low alloy steels in seawater. And the continuous rules of the samples’corrosion rate changing during exposure have been obtained. The results of carbon steels and low alloy steels immersed samples exposed for 1 and 2 years monitored by electrochemical methods is consistent with that of weight lost methods.
The relationships between corrosion rate of the samples and marine environmental factors (such as height of tide, temperature, velocity of seawater and orientation of flow) during the exposure have been studied by gray correlation analysis method. The results show that seawater temperature is the major factor influencing the corrosion rate of the samples exposed in immersed and tidal zone. The extent of tidal height influencing on the tidal zone samples is close to that of temperature.
The corrosion behaviors of 3C steel, 10CrMoAl steel, ZHMn55-3-1 copper alloy and HAl77-2 copper alloy have been investigated in different erosion-corrosion conditions of seawater with sand using simulated erosion-corrosion test systems. In the simulating marine velocity range of 0~0.8m/s, the main factor influencing on corrosion rate of 3C and 10CrMoAl steel is velocity of flow, the impact of silt content is not significant. In the test of simulating marine velocity and simulating high-speed erosion-corrosion, the velocity and silt all have an influence on the corrosion behaviors of ZHMn55-3-1 and HAl77-2 copper alloy.
The marine erosion-corrosion electrochemical detections of metallic materials have been achieved in Zhoushan marine corrosion test station. The results show that the corrosion rates of 3C steel, 10CrMoAl steel and ZHMn55-3-1 copper alloy augment with the velocity increasing in the velocity range of 1~3m/s, which is consistent with the results of weight lost methods. The erosion-corrosion appearances of materials have further verified the results of electrochemical detections.
实现了实海暴露金属试片的现场腐蚀电化学检测,恒电位方波和电化学阻抗谱(EIS)检测结果反映了试片在海水不同区带的腐蚀行为及海水环境因素的直接影响。确定了Q235钢、Q235超细晶钢、09CuPCrNiRE耐候钢和09CuPCrNi超细晶超高强度钢在海水中的极化阻力方程式的B值,为研究碳钢、低合金钢在海水中的腐蚀行为有很大意义。获得了实海试片暴露期间腐蚀速率的连续变化规律,碳钢、低合金钢全浸试片暴露1年和2年的电化学检测结果与失重结果一致。
采用灰关联分析法分析了暴露期间试片不同时间的腐蚀速度与海水环境因素(潮位、温度、流速和流向)的关系,结果表明:海水温度是影响全浸和潮差试片腐蚀速度的主要因素,海水潮位对潮差试片腐蚀速度的影响程度与温度的影响非常接近。
利用模拟冲刷腐蚀测试系统研究了3C、10CrMoAl、ZHMn55-3-1和HAl77-2在模拟泥沙海水冲刷条件下的腐蚀行为。模拟实海流速0~0.8m/s范围内,流速是影响3C和10CrMoAl腐蚀速度的主要因素,而泥沙含量的影响并不显著。流速和泥沙对ZHMn55-3-1和HAl77-2铜合金在模拟实海流速以及模拟高速下的冲刷腐蚀行为都有影响。
在舟山海水腐蚀试验站实现了金属材料的实海冲刷腐蚀电化学检测,检测结果表明:在流速1～3m/s范围内,3C、10CrMoAl和ZHMn55-3-1的腐蚀速度随流速的增加而增大,与实海冲刷腐蚀失重结果一致。材料的冲刷腐蚀形貌也进一步验证了电化学检测结果。
On the basis of China's material ambient seawater corrosion network test data accumulated, a great deal of valuable corrosion data has been obtained. National Natural Science Foundation of major projects "in situ material in a natural process of corrosion testing of new technology based on real-time monitoring and application" (No.50499335, 2004.9~2008.7), the main content of this project is "Water environment network typical metal corrosion specimens exposed real-time detection". Focused on the characteristics of Zhoushan seawater with larger concentration of sand and less marine organism, in field corrosion electrochemical detections of metal samples in Zhoushan marine corrosion test station have been implemented. The corrosion behaviors of metal samples both in simulated erosion-corrosion of seawater with sand and in marine erosion-corrosion conditions have been studied. These offer the foundation to investigate and forecast the corrosion performances of materials in marine environment.
The in field corrosion electrochemical detections of metal samples in marine environment have been achieved. Potentiostatic square wave and electrochemical impedance spectroscopy (EIS) results reflect the corrosion behaviors of metal samples exposed in different zone and the direct influence of marine environmental factors on the corrosion behaviors. The values of the parameter“B”in polarization resistance formula of Q235 carbon steel, Q235 ultrafine grained steel, 09CuPCrNiRE weathering steel and 09CuPCrNi ultrafine grained high strength steel have been identified, which have an great significance to investigate the corrosion behaviors o f carbon steels and low alloy steels in seawater. And the continuous rules of the samples’corrosion rate changing during exposure have been obtained. The results of carbon steels and low alloy steels immersed samples exposed for 1 and 2 years monitored by electrochemical methods is consistent with that of weight lost methods.
The relationships between corrosion rate of the samples and marine environmental factors (such as height of tide, temperature, velocity of seawater and orientation of flow) during the exposure have been studied by gray correlation analysis method. The results show that seawater temperature is the major factor influencing the corrosion rate of the samples exposed in immersed and tidal zone. The extent of tidal height influencing on the tidal zone samples is close to that of temperature.
The corrosion behaviors of 3C steel, 10CrMoAl steel, ZHMn55-3-1 copper alloy and HAl77-2 copper alloy have been investigated in different erosion-corrosion conditions of seawater with sand using simulated erosion-corrosion test systems. In the simulating marine velocity range of 0~0.8m/s, the main factor influencing on corrosion rate of 3C and 10CrMoAl steel is velocity of flow, the impact of silt content is not significant. In the test of simulating marine velocity and simulating high-speed erosion-corrosion, the velocity and silt all have an influence on the corrosion behaviors of ZHMn55-3-1 and HAl77-2 copper alloy.
The marine erosion-corrosion electrochemical detections of metallic materials have been achieved in Zhoushan marine corrosion test station. The results show that the corrosion rates of 3C steel, 10CrMoAl steel and ZHMn55-3-1 copper alloy augment with the velocity increasing in the velocity range of 1~3m/s, which is consistent with the results of weight lost methods. The erosion-corrosion appearances of materials have further verified the results of electrochemical detections.
引文
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