酸溶法大截面光纤传像束制备工艺及性能研究
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摘要
酸溶法工艺是当今世界制造光纤传像束的最先进的工艺技术。用酸溶法工艺制造的光纤传像束具有单丝直径细、柔性好、数值孔径大、分辨率高等优点，因此，它在医学、工业和军工等领域具有重要的应用价值，受到国内外的高度重视。
本文详细介绍了用酸溶法制造大截面光纤传像束的基本原理、工艺流程及技术方法，并对所研制的大截面光纤传像束的光学性能进行了测试，达到了实际使用的要求。本文采用一种先进的热熔工艺，将拉制的小截面酸溶法硬质光纤传像束截成一定长度后，经相关排列成大截面光纤传像束棒，然后经过热熔工艺和酸溶工艺，这样就制备出了酸溶法大截面光纤传像束。本实验所制备的大截面光纤传像束的直径为6.18mm，甚至还可以扩大，单丝直径为10μm，分辨率为42.5LP／mm。本文对影响酸溶法大截面光纤传像束性能的各种因素进行了分析，找出了诸多提高大截面光纤传像束性能的有效途径，最后探讨了热熔工艺对其性能的影响。
Today, the acid-leaching method is the best method to produce optical fiber image bundles in the wide world. The optical fiber image bundles produced by acid-leaching technique have the advantages of thinner diameter, good flexibility, larger numerical aperture and high-resolution etc. Therefore, they have an important application value in the medical, industrial and military areas. And it is highly regarded both at home and abroad.
In this dissertation, the basic principle, technical procedure and technical method, of preparing larger cross-section optical fiber image bundles by acid-leaching method were introduced in detail. And related tests were made for the optical performance of the prepared image bundles. In this dissertation, the advanced founding technique was used. By cutting prepared small cross-section optical fiber image bundles into certain length and being relatively sequenced into larger cross-section optical fiber image bundles, after founding technique and acid-leaching technique, the larger cross-section optical fiber image bundles in the acid-leaching method with diameter of 6.18mm or greater, diameter of single fiber of 8μm and resolution of 42.5Lp/mm were prepared. And then the influence factors on the performance of the larger cross-section optical fiber image bundles in the acid-leaching method were analysed in this dissertation. There were many methods how to improve the performance of image bundle were introduced. Finally, the influences that founding technique on performance were discussed.
本文详细介绍了用酸溶法制造大截面光纤传像束的基本原理、工艺流程及技术方法，并对所研制的大截面光纤传像束的光学性能进行了测试，达到了实际使用的要求。本文采用一种先进的热熔工艺，将拉制的小截面酸溶法硬质光纤传像束截成一定长度后，经相关排列成大截面光纤传像束棒，然后经过热熔工艺和酸溶工艺，这样就制备出了酸溶法大截面光纤传像束。本实验所制备的大截面光纤传像束的直径为6.18mm，甚至还可以扩大，单丝直径为10μm，分辨率为42.5LP／mm。本文对影响酸溶法大截面光纤传像束性能的各种因素进行了分析，找出了诸多提高大截面光纤传像束性能的有效途径，最后探讨了热熔工艺对其性能的影响。
Today, the acid-leaching method is the best method to produce optical fiber image bundles in the wide world. The optical fiber image bundles produced by acid-leaching technique have the advantages of thinner diameter, good flexibility, larger numerical aperture and high-resolution etc. Therefore, they have an important application value in the medical, industrial and military areas. And it is highly regarded both at home and abroad.
In this dissertation, the basic principle, technical procedure and technical method, of preparing larger cross-section optical fiber image bundles by acid-leaching method were introduced in detail. And related tests were made for the optical performance of the prepared image bundles. In this dissertation, the advanced founding technique was used. By cutting prepared small cross-section optical fiber image bundles into certain length and being relatively sequenced into larger cross-section optical fiber image bundles, after founding technique and acid-leaching technique, the larger cross-section optical fiber image bundles in the acid-leaching method with diameter of 6.18mm or greater, diameter of single fiber of 8μm and resolution of 42.5Lp/mm were prepared. And then the influence factors on the performance of the larger cross-section optical fiber image bundles in the acid-leaching method were analysed in this dissertation. There were many methods how to improve the performance of image bundle were introduced. Finally, the influences that founding technique on performance were discussed.
引文
1 刘德森等．纤维光学．北京：科学出版社，1987，19-25
2 张振远，孙磊，李莉等．集成大阵面光纤传像束实验研究．玻璃纤维，2004，4：1～6
3 孙磊．大截面光纤传像束及应用．玻璃纤维，1999，3：71～72
4 D. Marcuse. Theory of Dielectric Optical Waveguides.New York: Academic, 1994, 33～35
5 Djafar K. Mynbacv, Lowell L.Scheiner Fiber-Optic Communications Technology 影印版．北京：科学出版社，2002：50～51
6 廖延彪．光纤光学．北京：清华大学出版社，2000，3：1～18
7 张耀明．非通信光纤的研究及应用．玻璃纤维，1999，3：3～5
8 吴平，严映律．光纤与光缆技术．成都：西南交通大学出版社，2003：5
9 Lu Buyun, Yang Kewu,Xue Hongkui.2 meter length I R coherent bundle of As-Se-Te glass fibers. Infrared and Laset Enginee ring,2001,30(5):357～360
10 Pennington Tim othy L, Xiao Hai, Russell May. Miniaturize d 3-D surface profilometerusing a fiber optic coupler. Optics and Laser Technology, 2001,33:313～320
11 马养武．序排列光纤传像束光特性的测量研究．应用光学，1997，18(6)：36～40
12 孙圣和，王廷云，徐颖．光纤测量与传感技术．哈尔滨：哈尔滨工业大学出版社，2000，1：5～6
13 Cao Hui, Sun Junqiang, Chen Guojie, Huang Dexiu. Study on Unique Saturation Properties in Fiber Optical Parametric Amplifiers. ACTA PHOTONICA S1NCA,2005,34(2):225～229
14 Inoue K, Mukai T. Experimental Study on noise characteristics of a gain-saturated fiber optical parametric amplifier. J Lightwave Technol. 2002,20(1):969～974
15 李玉权，崔敏．光波导理论与技术．北京：人民邮电出版社，2002，12：44
16 Fan Guangzhao, Li Ruijun, Song Xinming. An Innovative Micro-3D Measurement System with Fiber Image Transm ission. Nanotechnology and Precision Engineering,2004,2(4):302～307
17 Zhou. A new definition for resolution of imaging fiber bundles a static scanning. Optik, 1993, 1:43
18 Yucheng Zhao, Katja, Lyytikainen, Martijn,Avan Eijkelenborg, Simon Smith. Nondestructive measurement of refractive index profile for holey fiber preform. 2003, 11:20～23
19 张振远，孙磊，李莉，张敏捷．基于层叠法工艺制造柔性多路集成大阵面光纤传像束实验研究．玻璃纤维，2004，4：1～5
20 徐明泉．光纤传像束的传光特性表征．光纤与光缆及其应用技术，1997，5：22～23
21 徐明泉，张振远，孔维彪等．光纤传像束的应用特点．光纤与光缆及其应用技术，1998，6：34～36
22 张振远，孙磊，李莉等．集成大阵面光纤传像束实验研究．玻璃纤维，2004，4：1～6
23 于凤霞，周艳艳，王新伟等．大数值孔径多组份玻璃非相干光纤材料的研究．吉林大学学报(工学版)，2003，10：47～49
24 于凤霞，周艳艳，于立亭等．大数值孔径多组份玻璃非相干柔性光纤的研究．中国激光，2004．31(4)：259～262
25 孙磊，陆小健．多组分玻璃纤维传像束的制造及检测．玻璃纤维，1999，3：45～47
26 Yu Zhu,Song Wei,He Guangyu. Effect of Single Fiber Core Diameter of Image-Carrying Optical Fiber Bundle on Optical Fiber Image Plane Hologram. Acta Optica Sinica.1997, 17(10):1341～1346
27 Yixin. Statistical of fiber bundle imagery of wavelevgth multiplexing. SPIE, 1994, 2302:244～252
28 胡先志．光纤的制造、性能及应用．技术，2001，2：23～24
29 蔡春平．拉丝条件对光纤折射率的影响．应用光学，2000，21(6)：25～29
30 于凤霞，柏昭辉，于立亭等．柔性光学纤维成像器件研究及传像特性分析．吉林大学学报(工学版)，2002，8：429～430
31 Komiyama.A, Hashimotom.M.A New Class of Crosstalk in Imaging Fibers.Optics Communications, 1994,6(107):49～53
32 Zhou. A new definition for resolution of imaging fiber bundles a static scanning. Optic, 1993, (1): 43
33 张文进．粘接技术在叠片法制造光纤传像束中的应用．粘结，1997，38～39
34 Ainhoa Gaston. optical fiber relative—humidity sensor with polyvinyl alcohol film[J]. applied optic.2004,21(7):4127～4132
35 扈性纯．酸溶法光纤传像束暗丝分析．应用光学，1998，19(10)：26～31
36 于凤霞，周艳艳，唐吉龙等．酸溶法光纤传象束暗丝问题研究．中国激光，2003，30：116～118
37 黄正中．玻璃的腐蚀与离子交换原理．光学技术，1980，(3)：18
38 武汉建材学院“玻璃工艺原理”建工出版社 1981
39 日本保谷厂技术报告“光学玻璃的腐蚀和化学组成的关系”．光学材料．1982，1：22
40 于凤霞等．酸溶法传象束工艺研究．光子学报．1999，28(Z1)：384～386
41 马养武．序排列光纤传像束光学特性的测量研究．光学仪器，1998，20(2)：31～35
42 Komiyama A, Hashimoto M. Electron Lett, 1989:25(16):1101～1103
43 扈性纯．酸溶法传像束工艺研究．光学纤维，1998，3：20～23
44 Liu Defu,Duan Jian.Mechanism research on lapping of optical fiber end-face. Optic and Precision Engineering,2004,12(6):570～575
45 LIN SHEN. Effect of polishing conditions on terminating optical connectors with spherical convex polished ends. Appl Opt, 2002, 41(1):88～95
46 UDREA M, ORUN H, ALACAKIR A. Laser polishing of optical fiber end surface. Optical Engineering, 2001, 40(9):2026～2030
47 张振远，徐明泉，孔维彪等．光纤传像监控系统的象质改进．玻璃纤维，2001，6：35～37
48 徐明泉，陆小健．光纤传像束极限分辨率的测试．玻璃纤维，1999，3：56～58
49 Ma Yangwu. Image trans mission performance of flexible fiber bundles. Laser Technology, 1999, 23(1):53～56
50 郁道银，谈恒英．工程光学．北京：机械工业出版社，1999：157～160
2 张振远，孙磊，李莉等．集成大阵面光纤传像束实验研究．玻璃纤维，2004，4：1～6
3 孙磊．大截面光纤传像束及应用．玻璃纤维，1999，3：71～72
4 D. Marcuse. Theory of Dielectric Optical Waveguides.New York: Academic, 1994, 33～35
5 Djafar K. Mynbacv, Lowell L.Scheiner Fiber-Optic Communications Technology 影印版．北京：科学出版社，2002：50～51
6 廖延彪．光纤光学．北京：清华大学出版社，2000，3：1～18
7 张耀明．非通信光纤的研究及应用．玻璃纤维，1999，3：3～5
8 吴平，严映律．光纤与光缆技术．成都：西南交通大学出版社，2003：5
9 Lu Buyun, Yang Kewu,Xue Hongkui.2 meter length I R coherent bundle of As-Se-Te glass fibers. Infrared and Laset Enginee ring,2001,30(5):357～360
10 Pennington Tim othy L, Xiao Hai, Russell May. Miniaturize d 3-D surface profilometerusing a fiber optic coupler. Optics and Laser Technology, 2001,33:313～320
11 马养武．序排列光纤传像束光特性的测量研究．应用光学，1997，18(6)：36～40
12 孙圣和，王廷云，徐颖．光纤测量与传感技术．哈尔滨：哈尔滨工业大学出版社，2000，1：5～6
13 Cao Hui, Sun Junqiang, Chen Guojie, Huang Dexiu. Study on Unique Saturation Properties in Fiber Optical Parametric Amplifiers. ACTA PHOTONICA S1NCA,2005,34(2):225～229
14 Inoue K, Mukai T. Experimental Study on noise characteristics of a gain-saturated fiber optical parametric amplifier. J Lightwave Technol. 2002,20(1):969～974
15 李玉权，崔敏．光波导理论与技术．北京：人民邮电出版社，2002，12：44
16 Fan Guangzhao, Li Ruijun, Song Xinming. An Innovative Micro-3D Measurement System with Fiber Image Transm ission. Nanotechnology and Precision Engineering,2004,2(4):302～307
17 Zhou. A new definition for resolution of imaging fiber bundles a static scanning. Optik, 1993, 1:43
18 Yucheng Zhao, Katja, Lyytikainen, Martijn,Avan Eijkelenborg, Simon Smith. Nondestructive measurement of refractive index profile for holey fiber preform. 2003, 11:20～23
19 张振远，孙磊，李莉，张敏捷．基于层叠法工艺制造柔性多路集成大阵面光纤传像束实验研究．玻璃纤维，2004，4：1～5
20 徐明泉．光纤传像束的传光特性表征．光纤与光缆及其应用技术，1997，5：22～23
21 徐明泉，张振远，孔维彪等．光纤传像束的应用特点．光纤与光缆及其应用技术，1998，6：34～36
22 张振远，孙磊，李莉等．集成大阵面光纤传像束实验研究．玻璃纤维，2004，4：1～6
23 于凤霞，周艳艳，王新伟等．大数值孔径多组份玻璃非相干光纤材料的研究．吉林大学学报(工学版)，2003，10：47～49
24 于凤霞，周艳艳，于立亭等．大数值孔径多组份玻璃非相干柔性光纤的研究．中国激光，2004．31(4)：259～262
25 孙磊，陆小健．多组分玻璃纤维传像束的制造及检测．玻璃纤维，1999，3：45～47
26 Yu Zhu,Song Wei,He Guangyu. Effect of Single Fiber Core Diameter of Image-Carrying Optical Fiber Bundle on Optical Fiber Image Plane Hologram. Acta Optica Sinica.1997, 17(10):1341～1346
27 Yixin. Statistical of fiber bundle imagery of wavelevgth multiplexing. SPIE, 1994, 2302:244～252
28 胡先志．光纤的制造、性能及应用．技术，2001，2：23～24
29 蔡春平．拉丝条件对光纤折射率的影响．应用光学，2000，21(6)：25～29
30 于凤霞，柏昭辉，于立亭等．柔性光学纤维成像器件研究及传像特性分析．吉林大学学报(工学版)，2002，8：429～430
31 Komiyama.A, Hashimotom.M.A New Class of Crosstalk in Imaging Fibers.Optics Communications, 1994,6(107):49～53
32 Zhou. A new definition for resolution of imaging fiber bundles a static scanning. Optic, 1993, (1): 43
33 张文进．粘接技术在叠片法制造光纤传像束中的应用．粘结，1997，38～39
34 Ainhoa Gaston. optical fiber relative—humidity sensor with polyvinyl alcohol film[J]. applied optic.2004,21(7):4127～4132
35 扈性纯．酸溶法光纤传像束暗丝分析．应用光学，1998，19(10)：26～31
36 于凤霞，周艳艳，唐吉龙等．酸溶法光纤传象束暗丝问题研究．中国激光，2003，30：116～118
37 黄正中．玻璃的腐蚀与离子交换原理．光学技术，1980，(3)：18
38 武汉建材学院“玻璃工艺原理”建工出版社 1981
39 日本保谷厂技术报告“光学玻璃的腐蚀和化学组成的关系”．光学材料．1982，1：22
40 于凤霞等．酸溶法传象束工艺研究．光子学报．1999，28(Z1)：384～386
41 马养武．序排列光纤传像束光学特性的测量研究．光学仪器，1998，20(2)：31～35
42 Komiyama A, Hashimoto M. Electron Lett, 1989:25(16):1101～1103
43 扈性纯．酸溶法传像束工艺研究．光学纤维，1998，3：20～23
44 Liu Defu,Duan Jian.Mechanism research on lapping of optical fiber end-face. Optic and Precision Engineering,2004,12(6):570～575
45 LIN SHEN. Effect of polishing conditions on terminating optical connectors with spherical convex polished ends. Appl Opt, 2002, 41(1):88～95
46 UDREA M, ORUN H, ALACAKIR A. Laser polishing of optical fiber end surface. Optical Engineering, 2001, 40(9):2026～2030
47 张振远，徐明泉，孔维彪等．光纤传像监控系统的象质改进．玻璃纤维，2001，6：35～37
48 徐明泉，陆小健．光纤传像束极限分辨率的测试．玻璃纤维，1999，3：56～58
49 Ma Yangwu. Image trans mission performance of flexible fiber bundles. Laser Technology, 1999, 23(1):53～56
50 郁道银，谈恒英．工程光学．北京：机械工业出版社，1999：157～160