化工园区挥发性有机物现场红外光谱监测技术及应用
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- 英文论文题名：Application of Infrared Spectroscopy for Online Monitoring of Volatile Organic Compounds in Chemical Industry Park
- 论文作者：刘文清 ; 刘建国 ; 徐亮 ; 高闽光 ; 金岭 ; 李胜 ; 童晶晶 ; 魏秀丽 ; 李相贤
- 英文论文作者：Liu Wenqing ; Liu Jianguo ; Xu Liang ; Gao Minguang ; Jin Lin ; Li Sheng ; Tong Jingjing ; Wei Xiuli ; Li Xiangxian ; Anhui Institute of Optics and Fine Mechanics ; Chinese Academy of Sciences
- 年：2016
- 作者机构：中国科学院安徽光学精密机械研究所;
- 论文关键词：挥发性有机物 ; 污染源 ; 现场监测 ; 傅立叶变换红外光谱
- 英文论文关键词：VOCs ; environment impact ; monitoring technology ; FTIR spectroscopy
- 会议召开时间：2016-09-22
- 会议录名称：2016年中国环境与安全监测技术研讨会—第27届MICONEX2016科学仪器惠及民生系列分会场论文集
- 语种：中文
- 分类号：X831
- 学会代码：XDKX
- 会议名称：2016年中国环境与安全监测技术研讨会—第27届MICONEX2016科学仪器惠及民生系列分会场
- 会议地点：中国北京
- 主办单位：中国仪器仪表学会
- 学会名称：现代科学仪器编辑部
- 页数：8
- 文件大小：3064k
- 原文格式：D
- 会议级别：全国
摘要
中红外波段是主要气态污染物尤其是挥发性有机物(VOCs)的基频吸收带,大多数污染气体在该波段都有其特征光谱。傅立叶变换红外光谱技术是该波段的优选测量技术,它具有传统色散光谱技术难以同时具备的高分辨率、高信噪比和宽波段的特点,结合其多种形式的非接触测量方式,可以实现对气体的主被动监测,非常适合用于化工业园区的排放现场监测。我国在傅立叶变换红外光谱成套技术的自主研发方面取得了长足的进步,并形成了初具规模的应用系列和体系。本文讨论了傅立叶变换红外光谱的主要原理、技术方法和应用系统,并介绍了目前国内针对化工园区点、面源排放现场监测所开展的典型应用。
The mid-infrared region is the fundamental absorption band of the main gaseous pollutants, especially volatile organic compounds(VOCs). Most of the polluted gases have their characteristic spectra in this band. Fourier transform infrared spectroscopy is a preferred measurement technique for mid-infrared analysis. It has the advantages of high resolution, high signal-to-noise ratio and wide band which traditional dispersion technique cannot have them simultaneously. Combined with its many forms of non-contact measurement, it can be set up as active or passive system which is suitable for chemical industrial area emissions in-situ monitoring. In this paper, the theory, techniques and applications of Fourier transform infrared spectroscopy are discussed. The typical applications of chemical monitoring and monitoring of different sites are introduced.
The mid-infrared region is the fundamental absorption band of the main gaseous pollutants, especially volatile organic compounds(VOCs). Most of the polluted gases have their characteristic spectra in this band. Fourier transform infrared spectroscopy is a preferred measurement technique for mid-infrared analysis. It has the advantages of high resolution, high signal-to-noise ratio and wide band which traditional dispersion technique cannot have them simultaneously. Combined with its many forms of non-contact measurement, it can be set up as active or passive system which is suitable for chemical industrial area emissions in-situ monitoring. In this paper, the theory, techniques and applications of Fourier transform infrared spectroscopy are discussed. The typical applications of chemical monitoring and monitoring of different sites are introduced.
引文
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[4]刘建国,桂华侨,谢品华,等.大气灰霾监测技术研究进展.大气与环境光学学报,2015,(2):93~101
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[7]黄中华,王俊德.傅立叶变换红外光谱在大气遥感监测中的应用.光谱学与光谱分析.2002,22(2):235-238.
[8]Remote Sensing and Determination of Pollutants in Gas Plumes.Environmental Science&Technology.1973,7(5):417-423.
[9]R.Zander,G.Roland,L.Delbouille.Column Abundance and the Long-Term Trend of Hydrogen Chloride(HCl)above the Jungfraujoch Station.Journal of Atmospheric Chemistry.1987,5(4):395-404.
[10]R.Beer.Remote Sensing by Fourier Transform Spectrometry.First edition,New York:John Wiley,1992:1-144.
[11]J.Notholt,R.Neuber,O.Schrems,T.v.Clarmann.Stratospheric Trace Gas Concentrations in the Arctic Polar Night Derived by FTIR-spectroscopy with the Moon as IR Light Source.Geophysical Research Letters.1993,20(19):2059-2062.
[12]M.Hilton,A.H.Lettington,I.M.Mills.Passive Remote Detection of Atmospheric Pollutants using Fourier Transform Infrared(FTIR)Spectroscopy.SPIEProc.1993,2089:314-315.
[13]K.Sch?fer,R.Haus,J.Heland,A.Haak.Measurements of atmospheric trace gases by emission and absorption spectroscopy with FTIR.Berichte der Bunsen-Gesellschaft.1995,99(3):405-411.
[14]D.Sp?nkuch,W.D?hler,J.Güldner,A.Keens.Ground-based passive atmospheric remote sounding by FTIR emission spectroscopy:First results with EISAR.Contributions to Atmospheric Physics.1996,69(1):97-111.
[15]D.F.Flanigan.Detection of Organic Vapors with Active and Passive Sensors:A Comparison.Applied Optics.1986,25(23),4253-4260.
[16]A.Beil,R.Daum,R.Harig,G.Matz.Remote Sensing of Atmospheric Pollution by Passive FTIRSpectrometry.SPIE Proc.1998,3493:32-43.
[17]X.Liu,F.J.Murcray,D.G.Murcray.Comparison of HF and HCl Vertical Profiles from Ground Based High-Resolution Infrared Solar Spectra with Halogen Occultation Experiment Observations.Journal of Geophysical Research.1996,101(D6):10175-10181.
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[21]E.Mahieu,R.Zander,L.Delbouille,P.Demoulin,G.Roland,C.Servais,Observed Trends in Total Vertical Column Abundances of Atmospheric Gases from IRSolar Spectra Recorded at the Jungfraujoch,Journal of Atmospheric Chemistry.1997,28(1-3):227-243.
[22]F.J.Murcray,J.J.Kosters,R.D.Blatherwick,J.Olson,D.G.Murcray.High Resolution Solar Spectrometer System for Measuring Atmospheric Constituents.Applied Optics.1990,29(10):1520-1525.
[23]R.Sussmann,K.Schaefer.Infrared Spectroscopy of Tropospheric Trace Gases:Combined Analysis of Horizontal and Vertical Column Abundances.Applied Optics.1997,36(3):735-741.
[24]C.Oppenheimer,P.Bani,J.A.Calkins,M.R.Burton,G.M.Sawyer.Rapid FTIR Sensing of Volcanic Gases Released by Strombolian Explosions at Yasur Volcano,Vanuatu.Applied Physics B:Lasers and Optics.2006,85(2-3):453-460.
[25]W.F.Herget.Remote and Cross-stack Measurement of Stack Gas Concentrations Using a Mobile FTIR System.Applied Optics.1982,21(4):635-641.
[26]R.Haus,K.Schaefer,W.Bautzer,J.Heland,H.Mosebach,H.Bittner,T.Eisenmann.Mobile Fourier Transform Infrared Spectroscopy Monitoring of Air Pollution.Applied Optics.1994,33(24):5682-5689.
[27]T.Mori,K.Notsu.Remote CO,COS,CO2,SO2 and HCl Detection and Temperature Estimation of Volcanic Gas.Geophysical Research Letters.1997,24(16):2047-2050.
[28]C.Oppenheimer,P.Francis,M.Burton,A.J.H.Maciejewski,L.Boardman.Remote Measurements of Volcanic Gases by Fourier Transform Infrared Spectroscopy.Applied Physics B:Lasers and Optics.1998,67(4):505-515.
[29]P.Francis,C.Chaffin,A.Maciejewski,C.Oppenheimer.Remote Determination of Si F4 in Volcanic Plumes:A New Tool for Volcano Monitoring.Geophysical Research Letters.1996,23(3):249-252.
[30]J.Heland,K.Schfer.Analysis of Aircraft Exhausts with Fourier-transform Infrared Emission Spectroscopy.Applied Optics.1997,36(21):4922-4931.
[31]J.Heland,K.Sch?fer.Determination of major combustion products in aircraft exhausts by FTIRemission spectroscopy.Atmospheric Environment.1998,32(18):3067-3072.
[32]D.F.Flanigan.Prediction of the Limits of Detection of Hazardous Vapors by Passive Infrared with the use of Modtran.Applied Optics.1996,35(30):6090-6098.
[33]K.A.Mc Gee,T.M.Gerlach.Airborne Volcanic Plume Measurements Using an FTIR Spectrometer,Kilauea Volcano,Hawaii.Geophysical Research Letters.1998,25(5):615-618.
[34]H.Kobayashi,A.shimota,K.Kondo.Development and Evaluation of the Interferometric Monitor for Greenhouse Gases:a High-throughput Fourier-transform Infrared Radiometer for Nadir Earth Observation.Applied Optics.1999,38(33):6801-6807.
[35]C.Clerbaux,P.Chazette,J.Hadji-Lazaro,G.Mégie,J.-F.Müller,S.A.Clough.Remote Sensing of CO,CH4,and O3 using a Space Borne Nadir-viewing Interferometer.Journal of Geophysical Research.1998,103(D15):18999-19013.
[36]K.G.Gribanov,V.I.Zakharov,S.A.Tashkun,Vl.G.Tyuterev.A new software tool for radiative transfer calculations and its application to IMG/ADEOS spectra.Journal of Quantitative Spectroscopy&Radiative Transfer.2001,68(4):435-451.
[37]V.S.Connors,D.R.Cahoon,H.G.Reichle Jr.,H.E.Scheel.Comparison Between Carbon Monoxide Measurements from Spaceborne and Airborne Platforms.Canadian Journal of Physics.1991,69(8-9):1128-1137.
[38]A.Shimota,H.Kobayashi,S.Kadokura.Radiometric Calibration for the Airborne Interferometric Monitor for Greenhouse Gases Simulator.Applied Optics.1999,38(3):571-576.
[39]C.Clerbaux,J.Hadji-Lazaro,S.Payan,C.CamyPeyret,J.Wang,D.P.Edwards,M.Luo.Retrieval of CO from Nadir Remote Sensing Measurements in the Infrared by use of Four Different Inversion Algorithms.Applied Optics.2002,41(33):7068-7078.
[40]H.Worden,R.Beer,C.P.Rinsland.Airborne Infrared Spectroscopy of 1994 Western Wildfires.Journal of Geophysical Research.1999,102(D1):1287-1299.
[41]R.Sussmann,K.Schaefer.Infrared Spectroscopy of Tropospheric Trace Gases:Combined Analysis of Horizontal and Vertical Column Abundance.Applied Optics.1997,36(3):735-741.
[42]Goody R.M.,Yung Y.L..Atmospheric Radiation.England:Oxford University Press,1989:125-187.
[43]Griffiths P.R.,Haseth de J..Fourier Transform Infrared Spectroscopy,Wiley&Sons,New York,1986.
[44]Anderson R.J.,Griffiths P.R..Errors in Absorbance Measurements in Infrared Fourier Transform Spectrometry because of Limited Instrument Resolution[J].Analytical Chemistry,1975,47(14):2339-2347.
[45]徐亮.大气痕量气体的主动FTIR光谱分析方法及应用研究:[D].北京:中国科学院研究生院,2007.
[46]Berry R J,Hart B K,Richadson R L,et al.A lowresolution spectrometer for open-path Fourier-transform infrared spectrometry[J].Field Analytical Chemistry and Technology,1999,3(2):131~138
[47]Griffith D W T,Jamie I M.Fourier-transform infrared spectrometry in Atmospheric and Thance Gas Analysis,in Encyclopedia of Analytical Chemistry[M].Ed.By Meyers R A,Chichester:John Wiley&Sons,2000:1979
[48]徐亮,高闽光,刘建国,等.北京奥运期间石化工业区多组分污染气体的开放光程FTIR监测[J].大气与环境光学学报,2009,4(5):376~381
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