Determination of 15 Impurity Elements in Quartz Sand by Inductively Coupled Plasma-Atomic Emission Spectrometry
详细信息
- 责任者：Wei Jingjing (College of Chemistry and Chemical Engineering ; Ocean University of China ; Qingdao 266003 ; China) ; Xue Qiuhong
- 刊名：Rock and Mineral Analysis
- 出版年：2011
- 卷期：30(3)
- 关键词：ICP—AES ; inductively coupled plasma atomic emission spectroscopy ; 石英砂 ; quartz sand
- 页码：p.310-314
- 图表：5 tables, 27 refs.
- 分类号：0900
- 出版序号：924
- issnNo：ISSN0254-5357
- isbnNo：CN11-2131/TD
摘要
A method was developed to determine of Fe, Ti, Mg, Mn, Zn, Cu, Pb, As, Cd, Ni, Cr, Co, Sb, Al and Ba in the quartz sand by inductively coupled plasma-atomic emission spectrometry (ICP-AES). The effect of the HF-HClO4 and HF-H2SO4 digestion systems to the results was investigated. Moreover, the conditions of acid consumption, digestion temperature and instrumental conditions were optimized. The detection limits for the elements were 0.17～0.88 μg/g and the recoveries of the method were 90.4%～110.7% with RSD (n=6) of less than 5.0%. The method possesses the advantages of simple operation, high sensitivity, good precision and is suitable for routine analysis of impurity elements in the quartz sand.